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Chemical Analysis and Life Science Branch



NMR Room
Room No.160, BLDG 22

ECZ700R

JNM-ECZ700R
Magnet Superconducting Magnet (16.45 Tesla)
Method Pulse Fourier Transformation
Method of Stabilization of Magnetic Field Internal Lock with Auto SHIM
Sensitivity 400 for 13C
Detectable Nucleus 1H, others

Room No.316, BLDG 22

AV500
AVANCEIII 500US
Cryo Probe
Magnet Superconducting Magnet
(11.7 Tesla)
Method Pulse Fourier Transformation
Method of Stabilization
of Magnetic Field
Internal Lock
with Auto SHIM
Resolution 0.6x10-9 for 13C
Sensitivity 2500 for 13C
Detectable Nucleus 1H, 13C

Room No.311, BLDG 22

AV400N
AVANCEIII 400
Nanobay
Magnet Superconducting Magnet
(9.4 Tesla)
Method Pulse Fourier Transformation
Method of Stabilization
of Magnetic Field
Internal Lock
with Auto SHIM
Resolution 0.5x10-9 for 13C
Sensitivity 190 for 13C
Detectable Nucleus 1H, others



Solid-State NMR Room
Room No.160, BLDG 22

ECA600II
JNM-ECA600II
Magnet Superconducting Magnet (14.1Tesla)
Method Pulse Fourier Transformation
Probes
3.2mmHXMAS
(Solid)
31P,7Li,11B,23Na,27Al,13C,
79Br,29Si,6Li,15N
8mmHXMAS
(Solid)
1H,31P,7Li,11B,23Na,27Al,13C,
79Br,207Pb,29Si,6Li
1mmHXMAS
(Solid)
1H,31P,7Li,11B,23Na,27Al,13C,
79Br,207Pb,29Si,6Li,15N(,14N)
3.2mmFGMAS
(Soft Material)
1H,13C,79Br
5mmX
(Solid/Wide Line)
31P,7Li,11B,23Na,27Al,13C,
79Br,29Si,2H,6Li,15N
5mmTH-GR
(Liquid/Diffusion)
1H,19F,7Li,
11B - 17O,15N

Room No.311, BLDG 22

Inova400plus
UNITY Inova-400plus
Magnet Superconducting Magnet (9.4Tesla)
Method Pulse Fourier Transformation
Probes
CP/MAS-1 (Solid) 2H - 31P
CP/MAS-2 (Solid) 15N - 31P
Wide line (Solid) 1H, 33S - 31P
5mm Multi (Liquid) 1H, 19F, 15N - 31P
10mm Multi (Liquid) 1H, 19F, 15N - 31P
5mm PFG and Indirect (Liquid) 1H, 15N - 31P





MS Room
Room No.223 & 302, BLDG 22

JMS S3000 HDMS GC/TOFMS

JMS-S3000 (JEOL)
Ionization Method MALDI
Mass Spectrometer TOF
Ion optical system Spiral type
Flight Distance 17 m
Mass Range m/z : 10 - 30,000
Mass Resolution ≥60,000 (FWHM, ACTH fragment 1 - 17 m/z : 2,093)
Mass Precision ≤1 ppm
Sensitivity 500 amol Angiotensin II (m/z : 1,046), s/n > 50
Measurement Mode Positive mode, TOF/TOF
Negative mode, TOF/TOF
MS/MS Option MS-50610TT (JEOL)
Flight Distance 1.6 m
Mass Resolution ≥2,000 (FWHM)
Sensitivity 5 fmol Angiotensin II (m/z : 1,046), s/n > 20
Mass Precision ≤0.1 Da
Select Range for Precursor Ion m/z : 100 - 4,000
Synapt G2 HDMS (Waters)
Ionization Method ESI, APCI, ASAP, nanoflow ESI
Mass Spectrometer Quadropole, TOF Hybrid MS/MS
Ion optical system Reflectron type
Mass Range m/z : 20 - 100,000
Mass Resolution ≥40,000 (FWHM, m/z : 1,431)
Mass Precision ≤1 ppm
Sensitivity 50 pmol Leucine enkephalin (m/z : 556)
Measurement Mode Positive mode, MS/MS, MS/MS/MS
Negative mode, MS/MS, MS/MS/MS
GCT Premier (Waters)
Ionization Method EI, CI
Mass Spectrometer TOF
Ion optical system Reflectron type
Flight Distance 1.2 m
Mass Range m/z : 14 - 4,000
Mass Resolution ≥7,000 (FWHM, m/z : 614)
Mass Precision ≤5 ppm
Sensitivity 1 pg HCB (m/z : 283.8), s/n > 10 (EI)
Measurement Mode Positive mode / Negative mode
Vario EL cube (Elementar)
Sample Weight Organic Materials : ≤50 mg
Soil : ≤1 g
Range C : ≤40 mg
H : ≤3 mg
N : ≤15 mg
S : ≤6 mg
Measurement Time 10 min. (C,H,N,S)
Precisioin ≤0.1 %abs.
Calibration Curve Multi point Method




TA Room
Room No.314, BLDG 22

TAS300

TG8101D (RIGAKU) TG8120 (RIGAKU)
Range of Temperature r.t. - 1,300 oC r.t. - 1,300 oC
Sample Weight ≤500 mg ≤1 g
Range of TG ±0.1 - ±250 mg / fullscale ±0.1 - ±250 mg / fullscale
Resolution 1 µmg 0.1 µg
Range of DTA ±1.5 - ±1000 µV / fullscale ±1.5 - ±1000 µV / fullscale
DSC-8230L (RIGAKU) DSC-8230(EVO) (RIGAKU)
Range of Temperature r.t. - 725 oC, -150 - 200 oC r.t. - 725 oC
Range of DSC ±0.1 - ±100 mW / fullscale ±0.1 - ±100 mW / fullscale




ESR Room
Room No.306, BLDG 22

JES-FA200
JES-FA200

FA-200 JES-RE1X
Sensitivity 7x109 spins/0.1 mT 1x1011 spins/0.1 mT
Frequency 8.75 - 9.65 GHz 8.8 - 9.6 GHz
Microwave Power 0.1 µW - 200 mW 0.1 µW - 200 mW
Magnetic Field -100 - 1300 mT 0 - 650 mT





FT-IR/Raman Room
Room No.310, BLDG 22

NRS-3300

FT/IR-6300,IRT-5000
Range 400 - 7,800 cm-1
Accessory for Measurement transmission measurement
ATR
Micro spectroscopy [ 650 - 6,000 cm-1 ]
Tablets forming machines
NRS-3300
Range 50 - 8,000 cm-1
Laser 532.08 nm, 632.80 nm
Lense x5, x20, x50, x100, x20(for macro)
Diffraction grating 600, 1,800, 2,400 gr/mm





Material Dynamics Analysis Room
Room No.413, BLDG 22



DMS6100
Range of Temperature -150 - +600 oC
Range of Frequency 0.01 - 200 Hz
TMA/SS7100C
Range of Temperature -150 - +600 oC
Resolution 0.01 µm
Load Range ±5.8 N
Sample Size ≤25 mm
DSC8000
Range -170 - +750 oC
Precision ≤±0.03 %
Accuracy ±0.2 %
Programming Rate ≤±750 oC / min
minispec mq
Range of Temperature -100 - +200 oC
Frequency 20 MHz
Stability of Magnet ±00.1 oC (at 40 oC)





ICP Room
Room No.317, BLDG 22

ICPE-9000



ICPE-9000
MAX Frequency 1.6 kW
Stability of Output ≤±0.3 %
Range of Wavelength 167 - 800 nm
Resolution ≤0.005 nm @ 200 nm





Life Science Lab.
Room No.109, BLDG 22

iTC200

iTC200
Volume 0.2 ml
Range of Temperature 2 - 80 oC
Titration Volume 0.1 - 40 µl
Response Time 7 sec.




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